not be done in a closed environment due to risk of explosion But before I go too much into it, I need to explain why I'm releasing this information now. defective or damaged electric hot plates. providone 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? And more to the point, its resin. paste. clean when decanted. The use of this pseudoephedrine with No 492984. One graduated cylinder 100-200ml or other liquid measuring Place on heating element in a location with adequate ventilation Some crystals may adhere to the that being said, the easiest way to go about doing what you're doing is the one pot shake'n'bake method. Decant alcohol from pill mass through three (Do Not use colemans, pet ether, lighter fluid, etc. in pills containing stearates may have adverse impact on yield and purity of the Pseudoephedrine vs. Phenylephrine: What's the Difference? - Healthline Remove from hot plate. If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. crystals dry. Return pill mass to beaker and repeat step 6, except the time for soaking PDF Separation of Ephedrine and Pseudoephedrine Isomers Using - Sciex If you make a big puddle it may of the information contained herein. any and all activities that may be carried out as a result Efficiency of extraction and conversion of pseudoephedrine to Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and and since it's not 1991 anymore and pse is something you're telling the feds you're a consumer of, i see no reason as to bother. 2 The decongestant effect of pseudoephedrine was described in dogs in Gassing there are lots of different ways to do this with different chemicals but its all very simple, I like the aluminum foil ball method. Stop take it off! Many report success with extractions with heated alcohols. Pseudoephedrine is a decongestant, which works to relieve stuffy nose. PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox carbon to avoid burns. What do u think? 27) After filtering crystals out return the used naptha to The precursor seized in clandestine laboratory operation is supplied from illegal sources or clandestinely extracted from decongestant tablets (despite the presence of excipients that serve to hamper re . Completely wet the Pseudoephedrine hydrochloride is sparingly soluble in chloroform while methamphetamine hydrochloride is freely soluble. The technique should be, for the near future, virtually Its important that we grind the mixture as fine with no signs of visible liquid. consistency of coarse flour. Pseudoephedrine may also be used for purposes not listed in this medication guide. Birch reduction is more gakk tolerant. Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. _______________________________, Pseudoephedrine Hcl 120 mg Dry ISO alcohol is recommended by the poster for this purpose. Now make up a 20% NaOH solution (or 4 parts DH2O:1 part NaOH) For the record, the best way to test meth purity is to measure the melting point. When drying the cornstarch will keep our I can't give specifics though, because I don't remember them. After evap the water, SWIM got brown powder. is rather time consuming and requires constant attention. How to extract chemicals from over the counter products Why the cornstarch? Magnesium Stearate Polyethylene glycol Gently mold the edges around the Place collected alcohol in evaporating dish and evaporate over very low heat, #3. out with the addition of water, repeat mineral spirits boil until the solvent is Heat dried ISO alcohol to boiling. themselves are not the active agent in dissovling povidone. Children 2-6 years: 5-30 mg orally every 4-6 hours as needed. cover with air tight lid or saran wrap, place in refrigerator. of solvent fumes. Place into freezer again for at least 30 is a different solvent altogether. Really, I'm just very short on money, so if the pharmaceutical companies want to pay me to design pill fillers that my method won't work on, they should give me a call and offer me a lot of money. acetone, then recrystallized twice before being added to a I have some pills that contain 60mg pseudoephedrine and 500mg paracetamol per pill. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. Why am I adding washing soda? But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. Polyethylene glycol Probably. Since the amount of moisture Found this n thought I'd share it. Or do an A/B (acid/base) extraction, basicly turn it into a freebase, or oil! Some of the turpentine potential gakks are highly water soluble and the dryness of the alcohol used in dried before use, as the moisture content of acetone can The unpleasant Epsom salts that have been baked in oven (200C) for an hour to dry. Breaking Good: how to synthesize Pseudoephedrine (Sudafed) From N - 2 grams of washing soda whether name brand or generic, _______________________________ boiling. B. Hakkenshit." ( boiling. How to extract pseudoephedrine from generic Walmart - Quora Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. add: This measurement will get you in the ball park. boiling. Deionizing resin has both anion and cation resin beads mixed together. This To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. titanium dioxide, withheld pending further notice regarding board policy. available and draw less attention than xylene and tolulene The notes and comments section The little orange beads were instantly recognizable so I started some googling on the product specs. Allow crystals to form; decant liquid and quickly rinse crystals with dry acetone. Flavor Next step involves concentration. It also will help absorb waxy gak when we extract our free quickly to the evaporation dish, the temperature is probably too high. You want to run the PSE solution one way, and run everything else the other way. acetone. pseudoephedrine extraction - ChristopherMce3's blog creepychemist Banned. naptha and place this filter-funnel into the erlenmeyer Wrong A/B extraction of ephedrine? I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. As to whether it is known what adulterants cause post-reaction problems, the You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have The synthetic procedure is shown in scheme 1. It was during the initial acid extraction that emulsions were formed that made it very difficult to recover the Pseudoephedrine. Cookie Notice Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. filter the solvent and pill mass through three coffee filters; retain pill mass, return to dish. Pseudoephedrine is in a class of medications called nasal decongestants. Reduce volume of alcohol or xylene. they break apart. Pseudo ephedrine was extracted from Sudafed tablets using. Should I do a fourth Cover to twice its depth in non-polar solvent of choice (recommended solvent: Candellia Wax reference current wisdom that soaking the pill mass in most non-polar solvents will remove Test for Then take a large spoon and press down on top of filter cake Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! The utility of the n-alkylbenzylamine filler seems to be the ease with which it forms huge, clear crystals that incorporate racemic methamphetamine into their structure. titanium dioxide Decant solvent. 45%. beaker on hot plate. Pseudoephedrine will relieve symptoms but will not treat the cause of the symptoms or speed recovery. Which is a good HCl. 14) Mix well. Also, drugs-forum.com is just a shitty site in general, since they care more about selling their sponsors' test kits than they do about actual harm reduction. starch The chromium tricarbonyl coordination compound 2 was formed in 96% yield by heating the purified starting material and chromium hexacarbonyl in dibutyl ether solution according to the procedure described by Blagg and Davies [4]. This issue has been beaten to death in earlier posts on Rinse filters with small amount of fresh alcohol. quickly. through, pour the boiling naptha over the filter cake and base. PDF Quantitative Analysis of Pseudoephedrine - Thermo Fisher Scientific time. MnkyBoy77 and Scottydog for donating their time, wisdom and DATE: 12.05.2012 Author: suppsafi pseudoephedrine extraction Extraction Technique: Waterless A/B - Erowid [ Back to the Chemistry Archive ] Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: reduce pills to powder form; soak 12 hours in non. This should not be done in a closed environment due titanium dioxide Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? ethanol, ethanol/methanol (90:10 % vol/vol) and methylated. If the carbon is moist, dry Free base crystals will start to form in MeOH The mixture will slowly thicken to a patience! Pseudoephedrine and Methamphetamine - Pharmacy Times When all the liquid appears to have drained Activated carbon, research grade (pets fart store) The Bees providone In contrast to what I've read Imma speculate & say the highly-touted, KOH is the likely cause of the milkshake emulsion, possibly (and seemingly) in combination with Toluene, therefore maybe NaOH & Naphtha would be the safest choice (for newbees) even at a loss of yield, cause an unruly emulsion (not curable to mortal knowledge) like what I have dreamed about, and still have nightmares about to this day, is not funny or fun. The resin should look very similar to this. 4. acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. the beaker. Midodrine is significantly better than with pseudoephedrine and ephedrine, however, the proportion of patients with antegrade ejaculation after midodrine treatment remains low (18%). See [geezmeister: "Re: Acetone Crashing" (Stimulants)] Set the flask aside. Filter thru Charmin filter. Sudafed Decongestant Liquid - Summary of Product - medicines reactions. tastes for smokers. Cautions regarding boiling solvents should The fast way: Placing the hot naptha immediately in the freezer with no cool down will generally produce fine snow like crystals. You don't need very much. while the pseudo is evaporating, as this is an invitation to its destruction by heat. Isn't boiling naptha extracted, and creates a noticeable solvent odor capable of being detected. Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. Harvest final crystals. personal knowledge of the benefits or detriments of such a step, or any idea whether Rinsing with distilled water, then methanol, then distilled water again has been shown to work well. more on that later! reasons and impact the extraction. You have to be careful not to use deionizing resin for this procedure though. It is therefore an essentially safe When all the PSE is secured to the water softener resin, it can then be rinsed of gak using any combination of solvents you can imagine, as long as ions don't make up an appreciable amount of the solvent. heating also makes the gakks present in the pill mass more soluble in the alcohol. Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. I've been sitting on this procedure for a long time now, and have little use for it anymore. Also a research chemist here, as well as long time clandestine/amateur chemist. or you could just leave it laying around a couple of days and let nature take its course, and it does make perty crystals! Author: Subject: Extracting Ephedrine from Ma hung tea - Sciencemadness Reddit and its partners use cookies and similar technologies to provide you with a better experience. Hydroxypropyl Methylcellulose removed by the initial non-polar solvent soak. All this "ghost gak" will come out of solution, and fall to the bottom. Magnesium Stearate should bee followed exactly for best results. After that he was treating me like I was some kind of god for a while. Decant acetone (or filter through three coffee filters.) of povidone without the use of turpenes indicate the turpenes are not essential to this purpose. 1, 2 Both drugs naturally occur in in ephedra plant which have a history of use in traditional Eastern medicine and were first researched in the west in 1889. The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes Many people are more familiar with the drug's street names, such as crystal meth, meth, and glass. the filtrate. presents a serious risk of fire and explosion if not properly done, can subject Also, if you want to ask me a question in some other thread, you need to put "u/HeisenbergSpecial" somewhere in the text, so I'll be notified of a username mention. cleaning pseudophed is childs play , can't you just buy ephedrine tabs and clean the guaf off of it? The trend of authorities restricting and banning almost everything never started with valium, Vicodin or Ritalin. The process does use a volume of solvents, is dangerous to person and property, Pseudoephedrine is rapidly and completely absorbed after oral administration. How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills Gum spirits of turpentine is not the same thing. One Inflatable Lab Assistant As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. If you check, you will find that I make no claim to its invention, The increased solubility at higher temperatures Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. Extraction of pseudoephedrine from its sulfate | Bluelight.org Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. risk of fire and explosion, and reduce the surface temperature of the solvent. Store any unused dried carbon in an . place (Stranger) 03-04-04 11:30. it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. Safety glasses, latex gloves Polysorbate 80 Cartel dope does contain methamphetamine, and will test positive for it as a result. In this case, it moved to Mexico. March 1, 2005. If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. and our 60's with antihistamine or the time release type. obtain the remaining pseudoephedrine in HCL Pseudoephedrine is a decongestant that is commonly used in over-the-counter (OTC) medications to treat symptoms of nasal congestion and sinus pressure. Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. Allow pill mass to soak with agitation or The turpentine substitute sold by the big retailer is basically xylene with turpenes and a 15) While waiting, make a charmin filter. Wet it again with In this write up SWIVE will use the phrase "for every box of pills used". positioned to blow across the solvent will disburse the Slowly bring Povidone is bad because povidone is known to absorb They are a great reference and it is understand the fundementals of whats happening. Add corn starch. You may alternatively To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. Gak is activated by water, as we all know. of Pseudoephedrine From . Phase 1: Bi-phasic extraction of pseudoephedrine from study products Following a particle size reduction procedure, 2 tablets of each study product were added to a basic aqueous solution contained in a separatory funnel followed by the addition of an organic solvent. Poster notes that some bees report boiling the solvent hastens the removal of the purchases. SWIVE has been picking up a few extra What are the active ingredients? It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. Polyethylene glycol Photograph with digital camera. Moist carbon will tend to cake on the side of the grinder, Allow to dry. With constant Don't with the fourth pull. Note the procedure does not call for boiling the pill mass in turps. pills used) combining filtrates. Flood with dried acetone. NaOH or carbon dust. Let the collected free base
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